MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\BIZ\\BIZ2016-D06-WJ8.D Tgt Mass (EZX): 232.00 Injection Date : 6 Dec 16 11:47 am +0800 Seq. Line : 0 Sample Name : BIZ2016-D06-WJ8 Location : P1-D-07 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-100588 Batch#22718 Easy-Access Method: '1-POS-3MIN' 232.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU1500100050000.5*DAD1 C, Sig=254,4 Ref=off mAU60040020000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7040000030000020000010000000.511.5 Ion 233, MSD1 233,Target Mass 232 +H Positive, EIC=232.7:233.7 20000010000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.5221.9912.5min1.51.58711.51.6011.99521.9952.5min*21.9902.5min*2.3572.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.60 0.01 9.83 10.58 0.46 128 1.99 0.02 2122.33 2145.55 99.54 233 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.59 0.02 2.01 0.21 0.23 128 1.99 0.01 859.51 882.14 99.77 233HY-LCMS-02 12/6/2016 13:08:19 KFF(LCMS-02)Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.99 <<<< POSITIVE SPECTRA >>>> ES-API Positive90000800007000060000500004000020000100000200300400500600700800900m/z 234.130000 233.2HY-LCMS-02 12/6/2016 13:08:19 KFF(LCMS-02)Page 2 of 2
